Crystal chemistry of elpidite from Khan Bogdo (Mongolia) and its K- and Rb-exchanged forms

Autor(en)
A.A. Grigor’eva, Natalia V Zubkova, Igor V Pekov, Uwe Kolitsch, Dmitry Y. Pushcharovsky, Marina F. Vigasina, Gerald Giester, Tamara Đorđević, Ekkehart Tillmanns, N V Chukanov
Abstrakt

Elpidite Na2ZrSi6O15 3H2O [space group Pbcm, a = 7.1312(12), b = 14.6853(12), and c = 14.6349(15) .ANG.] from Khan Bogdo (Mongolia) and its K- and Rb-exchanged forms K1.78Na0.16H0.06ZrSi6O15 0.85H2O [Cmce, a = 14.054(3), b = 14.308(3), and c = 14.553(3) .ANG.] and Na1.58Rb0.2H0.22ZrSi6O15 2.69H2O [Pbcm, a = 7.1280(10), b = 14.644(3), and c = 14.642(3) .ANG.] that were obtained by cation exchange at 90C, as well as K1.84Na0.11H0.05ZrSi6O15 0.91H2O [Cmce, a = 14.037(3), b = 14.226(3), and c = 14.552(3) .ANG.] and Rb1.78Na0.06H0.16ZrSi6O15 0.90H2O [Cmce, a = 14.2999(12), b = 14.4408(15), and c = 14.7690(12) .ANG.], obtained at 150C are studied by single-crystal X-ray diffraction and IR spectroscopy. The base of the structures is a heteropolyhedral Zr-Si-O framework whose cavities accommodate Na (K, Rb) cations and H2O mols.

Organisation(en)
Institut für Mineralogie und Kristallographie
Externe Organisation(en)
Lomonosov Moscow State University (MSU), Naturhistorisches Museum Wien (NHM), Russian Academy of Sciences
Journal
Crystallography Reports
Band
56
Seiten
832-841
Anzahl der Seiten
10
ISSN
1063-7745
Publikationsdatum
2011
Peer-reviewed
Ja
ÖFOS 2012
105113 Kristallographie
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/0ae21461-0bd5-4b9a-a4b9-87e62f3630bc