Mixed salt of sarcosine containing dimeric undecafluoridodialuminate anion and fluoride ion

Autor(en)
Gerald Giester, V. V. Ghazaryan, Subbiah Thamotharan, María Judith Percino, Aram M. Petrosyan
Abstrakt

We report on synthesis, structural and vibrational spectroscopic characterization of the (SarH) 6[F5Al- F- AlF5] F (I) salt. The compd. (I) is the first salt of amino acids with a dimeric undecafluoridodialuminate [F5Al- F- AlF5] 5- anion and the first mixed salt of sarcosine with different anions. It crystallizes in orthorhombic system, space group Pbca. The simulated FT- IR spectrum for a cluster which comprises 13 cations, [F5Al- F- AlF5] 5- anion and a fluoride anions built from the crystal structure is compared with the exptl. spectrum and agree reasonably well.

Organisation(en)
Institut für Mineralogie und Kristallographie
Externe Organisation(en)
Shanmugha Arts, Science, Technology & Research Academy, Benemérita Universidad Autónoma de Puebla, National Academy of Sciences of the Republic of Armenia
Journal
Journal of Fluorine Chemistry
Band
209
Seiten
73-78
Anzahl der Seiten
6
ISSN
0022-1139
DOI
https://doi.org/10.1016/j.jfluchem.2018.02.011
Publikationsdatum
02-2018
Peer-reviewed
Ja
ÖFOS 2012
104015 Organische Chemie, 104026 Spektroskopie, 105113 Kristallographie
Schlagwörter
ASJC Scopus Sachgebiete
Biochemistry, Inorganic Chemistry, Physical and Theoretical Chemistry, Environmental Chemistry, Organic Chemistry
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/1f220d08-ae99-4a09-b4df-e71d22f3eaa7