Complexes of N-hydroxyethyl-N-benzimidazolylmethylethylenediaminediacetic acid with group 12 metals and vanadium-Synthesis, structure and bioactivity of the vanadium complex

Autor(en)
Ladislav Habala, Caroline Bartel, Gerald Giester, Michael A. Jakupec, Bernhard K. Keppler, Annette Rompel
Abstrakt

Four new complexes of group 12 metals [Zn(II), Cd(II) and Hg(II)], along with vanadyl bound to the ligand N-hydroxyethyl-N-benzimidazolylmethylethylenediaminediacetic acid, have been synthesized and characterized. The structure of the complexes with Zn(II), Hg(II) and V(IV) was determined by X-ray structural analysis. In all observed cases, the symmetry of these complexes was found to be distorted octahedral. The inhibition of protein tyrosine phosphatase 1B by the vanadium(IV) complex was demonstrated. The cytotoxicity of the vanadium(IV) complex was tested in vitro against three cancer cell lines, with a comparison of the activity of the free ligand and of vanadyl acetylacetonate and sodium orthovanadate. The IC

50 values of the complex were in the range of 9 to 21 μM. Remarkably, cytotoxic potency in the multidrug-resistant non-small cell lung cancer cell line A549 was at least as high as in the broadly chemosensitive ovarian teratocarcinoma cell line CH1(PA-1).

Organisation(en)
Institut für Biophysikalische Chemie, Institut für Anorganische Chemie, Institut für Mineralogie und Kristallographie
Journal
Journal of Inorganic Biochemistry
Band
147
Seiten
147-152
Anzahl der Seiten
6
ISSN
0162-0134
Publikationsdatum
04-2015
Peer-reviewed
Ja
ÖFOS 2012
104003 Anorganische Chemie, 106002 Biochemie, 105113 Kristallographie
Schlagwörter
ASJC Scopus Sachgebiete
Biochemistry, Inorganic Chemistry
Sustainable Development Goals
SDG 3 – Gesundheit und Wohlergehen
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/complexes-of-nhydroxyethylnbenzimidazolylmethylethylenediaminediacetic-acid-with-group-12-metals-and-vanadiumsynthesis-structure-and-bioactivity-of-the-vanadium-complex(383cbc5f-ee70-4bac-9c96-48382325e84d).html