Preparation and characterization of L‑cystinium(2+) bis‑iodide monohydrate and L‑cystinium(2+) bis‑triiodide

Autor(en)
Aram M. Petrosyan, Gerald Giester, Milena S. Petrosyan, Vahram V. Ghazaryan, Ashkhen L. Zatikyan
Abstrakt

Two new crystalline salts of L-cystine, [L-cystinium(2+) bis-iodide monohydrate (L-CsnH2)(I)2·H2O (I) and L-cystinium(2+) bis-triiodide (L-CsnH2)(I3)2 (II)], were obtained and characterized structurally, by vibrational spectroscopy and their electronic structure by quantum chemical calculations (CASTEP Package) in the framework of density functional theory (DFT).
The bandgap of (II) was also determined experimentally by diffuse reflectance spectroscopy. Both salts crystallize in the orthorhombic space group P212121. The composition and structure of (I) differ from those previously known chloride and bromide salts. A specific supramolecular anionic substructure was found in the structure of (II).

Organisation(en)
Institut für Mineralogie und Kristallographie
Externe Organisation(en)
National Academy of Sciences of the Republic of Armenia, Yerevan State University
Journal
Structural Chemistry
Anzahl der Seiten
12
ISSN
1040-0400
DOI
https://doi.org/10.1007/s11224-025-02495-6
Publikationsdatum
2025
Peer-reviewed
Ja
ÖFOS 2012
105116 Mineralogie, 105113 Kristallographie
Schlagwörter
ASJC Scopus Sachgebiete
Condensed Matter Physics, Physical and Theoretical Chemistry
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/a1314856-c664-4a70-af5f-8182aadbf063