Crystal structure of hexaglycinium dodecaiodotriplumbate

Autor(en)
Gayane S. Tonoyan, Gerald Giester, Vahram V. Ghazaryan, Ruben Yu. Chilingaryan, Arthur A. Margaryan, Artak H. Mkrtchyan, Aram M. Petrosyan
Abstrakt

The crystal structure of hexaglycinium tetra-µ-iodido-octaiodidotriplumbate,
(C2H6NO2)6[Pb3I12] or (GlyH)6[Pb3I12], is reported. The compound crystallizes
in the triclinic space group P1. The [Pb3I12]6- anion is discrete and located
around a special position: the central Pb ion located on the inversion center is
holodirected, while the other two are hemidirected. The supramolecular nature
is mainly based on C—H···I, N—H···I, O—H···I and N—H···O hydrogen
bonds. Dimeric cations of type (A+···A+) for the amino acid glycine are
observed for the first time.

Organisation(en)
Institut für Mineralogie und Kristallographie
Externe Organisation(en)
National Academy of Sciences of the Republic of Armenia
Journal
Acta Crystallographica. Section E: Crystallographic Communications
Band
80
Seiten
916-920
Anzahl der Seiten
5
ISSN
2056-9890
DOI
https://doi.org/10.1107/S2056989024007606
Publikationsdatum
09-2024
Peer-reviewed
Ja
ÖFOS 2012
105116 Mineralogie, 105113 Kristallographie
Schlagwörter
ASJC Scopus Sachgebiete
Condensed Matter Physics, Allgemeine Chemie, Allgemeine Materialwissenschaften
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/a616ce6c-c686-4d33-bd6b-51e710fc9c7b