Two three-dimensional coordination polymers of lead(II) with iminodiacetate and naphthalene-dicarboxylate anions: Synthesis, characterization and luminescence behavior

Autor(en)
Debdoot Hazari, Swapan Kumar Jana, Michel Fleck, Ennio Zangrando, Sudipta Dalai
Abstrakt

Two lead(II) compounds [Pb3(idiac)3(phen)2(H2O)]·2(H2O) (1) and [Pb(ndc)]n (2), where H2idiac=iminodiacetic acid, phen=1,10-phenanthroline and H2ndc=naphthalene-2,6-dicarboxylic acid, have been synthesized and structurally characterized. Single crystal X-ray diffraction analysis showed that compound 1 is a discrete trinuclear complex (of two-fold symmetry) which evolves to a supramolecular 3D network via π–π interactions, while in compound 2 the naphthalene dicarboxylate anion act as a linker to form a three dimensional architecture, where the anion adopts a bis-(bidentate bridging) coordination mode connecting four Pb(II) centers. The photoluminescence property of the two complexes has been studied.

Organisation(en)
Institut für Mineralogie und Kristallographie
Externe Organisation(en)
Vidyasagar University, Università degli Studi di Trieste
Journal
Journal of Solid State Chemistry
Band
219
Seiten
43-48
Anzahl der Seiten
6
ISSN
0022-4596
DOI
https://doi.org/10.1016/j.jssc.2014.07.004
Publikationsdatum
07-2014
Peer-reviewed
Ja
ÖFOS 2012
104015 Organische Chemie, 104021 Strukturchemie, 105113 Kristallographie
Schlagwörter
ASJC Scopus Sachgebiete
Electronic, Optical and Magnetic Materials, Condensed Matter Physics, Ceramics and Composites, Materials Chemistry, Inorganic Chemistry, Physical and Theoretical Chemistry
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/dcbd0f6f-4521-44e4-a46c-3926963a0703