Mixed salts of amino acids with different anions

Autor(en)
V. V. Ghazaryan, Michel Fleck, A.M. Petrosyan
Abstrakt

Mixed salts of amino acids with different anions are of considerable interest from chemical and structural points of view and also as a source of new materials the properties of which can be controlled by appropriate choice of anions. Four such crystals, L-His2+·Cl-·HSO4- (P212121, Z=4), L-Arg2+·NO3-·ClO4- (d-form, P21, Z=4), L-Arg2+·F-·NO3- (P1, Z=2), 2L-Arg2+·(F-?HF)·3NO3- (P212121, Z=4), have been characterized structurally and by IR and Raman spectra. The hydrogen bond between the carboxyl group and the fluoride ion (2.371(3) Å) in the structure of L-Arg2+·F-·NO3- is among the shortest known O-H?F type hydrogen bonds. The O-H?F hydrogen bond in the structure of 2L-Arg2+·(F-?HF)·3NO3- is even shorter (2.341(2) Å) and thus belongs to the shortest contacts among both ?–??F and F–-?O types hydrogen bonds.

Organisation(en)
Institut für Mineralogie und Kristallographie
Externe Organisation(en)
National Academy of Sciences of the Republic of Armenia
Journal
Journal of Crystal Growth
Band
362
Seiten
182-188
Anzahl der Seiten
5
ISSN
0022-0248
DOI
https://doi.org/10.1016/j.jcrysgro.2011.09.059
Publikationsdatum
2013
Peer-reviewed
Ja
ÖFOS 2012
105116 Mineralogie
Schlagwörter
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/e33f9700-428a-415f-abac-6f71127f9afe