Al-Ge-Ti: Phase equilibria and structural characterization of new ternary compounds

Autor(en)
Roland W. Bittner, Matthias Gürth, Liliana I. Duarte, Christian Leinenbach, Herta S. Effenberger, Klaus W. Richter
Abstrakt

Phase equil. of Al-?Ge-?Ti have been investigated using SEM (SEM)?, powder X-?ray diffraction (XRD) and DTA (DTA)?. Partial isothermal sections at 400 °C, 520 °C and 1000 °C were obtained with focus on the titanium-?poor part up to 50 at.?% titanium. Three ternary compds. were found to exist. The compd. Al3GeTi (t1) crystallizes in an own structure type (P4?/nmm, tP10)?. Two structurally closely related compds. were found at the compn. Al1-?xGe1+xTi: t2 (0.61 = x = 0.73)?, Al4Si5Zr3-?type, I41/amd, tI24 and t'2 (0.36 = x = 0.57)?, Si2Zr-?type, Cmcm, oC12. DTA data were used to construct a ternary reaction scheme (Scheil diagram) up to approx. 1300 °C, a partial liquidus projection and two vertical sections, at 10 at.?% Ti and at a const. Al:Ti ratio of 1:1. A total no. of 12 ternary invariant reactions were identified.

Organisation(en)
Institut für Funktionelle Materialien und Katalyse, Institut für Mineralogie und Kristallographie, Core Facility für Kristallstrukturanalyse
Externe Organisation(en)
Eidgenössische Materialprüfungs- und Forschungsanstalt
Journal
Intermetallics
Band
53
Seiten
157-168
Anzahl der Seiten
12
ISSN
0966-9795
DOI
https://doi.org/10.1016/j.intermet.2014.05.003
Publikationsdatum
05-2014
Peer-reviewed
Ja
ÖFOS 2012
104011 Materialchemie, 104003 Anorganische Chemie, 105113 Kristallographie
Schlagwörter
ASJC Scopus Sachgebiete
Mechanical Engineering, Mechanics of Materials, Materials Chemistry, Metals and Alloys, Allgemeine Chemie
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/ed63c8d4-d040-4ab1-86d2-ff1a8c7f001e