Synthesis of thieno[2,3-b]pyrazines via an acylation-deacylation process of 3,4-dihydro precursors

Autor(en)
Thomas Erker, Karin Trinkl, Franz Pertlik
Abstrakt

In the first step 3, 4-dihydrothieno[2,3-b]pyrazines (1, 2 and 4) were N-acylated by the acyl chlorides followed by a deacylation process mediated by triethylamine to give thieno[2,3-b]pyrazines. In a final rection the excess of the appropriate acyl chlorides react with the free hydroxy residue to afford compounds (15, 16 or 17).

Organisation(en)
Institut für Mineralogie und Kristallographie
Externe Organisation(en)
Universität Wien
Journal
Heterocycles
Band
60
Seiten
337-344
Anzahl der Seiten
8
ISSN
0385-5414
DOI
https://doi.org/10.3987/COM-02-9638
Publikationsdatum
2003
Peer-reviewed
Ja
ÖFOS 2012
3012 Pharmazie, Pharmakologie, Toxikologie
Link zum Portal
https://ucrisportal.univie.ac.at/de/publications/f4612285-eb1b-4bba-bcb3-300e702d8eaa