Mixed salt of sarcosine containing dimeric undecafluoridodialuminate anion and fluoride ion

Author(s)
Gerald Giester, V. V. Ghazaryan, Subbiah Thamotharan, María Judith Percino, Aram M. Petrosyan
Abstract

We report on synthesis, structural and vibrational spectroscopic characterization of the (SarH) 6[F5Al- F- AlF5] F (I) salt. The compd. (I) is the first salt of amino acids with a dimeric undecafluoridodialuminate [F5Al- F- AlF5] 5- anion and the first mixed salt of sarcosine with different anions. It crystallizes in orthorhombic system, space group Pbca. The simulated FT- IR spectrum for a cluster which comprises 13 cations, [F5Al- F- AlF5] 5- anion and a fluoride anions built from the crystal structure is compared with the exptl. spectrum and agree reasonably well.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
Shanmugha Arts, Science, Technology & Research Academy, Benemérita Universidad Autónoma de Puebla, National Academy of Sciences of the Republic of Armenia
Journal
Journal of Fluorine Chemistry
Volume
209
Pages
73-78
No. of pages
6
ISSN
0022-1139
DOI
https://doi.org/10.1016/j.jfluchem.2018.02.011
Publication date
02-2018
Peer reviewed
Yes
Austrian Fields of Science 2012
104015 Organic chemistry, 104026 Spectroscopy, 105113 Crystallography
Keywords
ASJC Scopus subject areas
Biochemistry, Inorganic Chemistry, Physical and Theoretical Chemistry, Environmental Chemistry, Organic Chemistry
Portal url
https://ucrisportal.univie.ac.at/en/publications/1f220d08-ae99-4a09-b4df-e71d22f3eaa7