An investigation of polyhedral deformation in two mixed-metal diarsenates: SrZnAs<sub>2</sub>O<sub>7</sub> and BaCuAs<sub>2</sub>O<sub>7</sub>

Author(s)
Sabina Kovac, Ljiljana Karanovic, Tamara Đorđević
Abstract

Two isostructural diarsenates, SrZnAs2O7 (strontium zinc diarsenate), (I), andBaCuAs2O7 [barium copper(II) diarsenate], (II), have been synthesized underhydrothermal conditions and characterized by single-crystal X-ray diffraction.The three-dimensional open-framework crystal structure consists of cornersharingM2O5 (M2 = Zn or Cu) square pyramids and diarsenate (As2O7) groups.Each As2O7 group shares its five corners with five different M2O5 squarepyramids. The resulting framework delimits two types of tunnels aligned parallelto the [010] and [100] directions where the large divalent nine-coordinated M1(M1 = Sr or Ba) cations are located. The geometrical characteristics of theM1O9 , M2O5 and As2O7 groups of known isostructural diarsenates, adoptingthe general formula M1IIM2IIAs2O7 (M1II = Sr, Ba, Pb; M2II = Mg, Co, Cu, Zn)and crystallizing in the space group P21/n, are presented and discussed.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
University of Belgrade
Journal
Acta Crystallographica. Section C: Crystal Structure Communications
Volume
C71
Pages
330-337
No. of pages
8
ISSN
0108-2701
DOI
https://doi.org/10.1107/S2053229615005616
Publication date
03-2015
Peer reviewed
Yes
Austrian Fields of Science 2012
104017 Physical chemistry, 104011 Materials chemistry, 105113 Crystallography
Keywords
ASJC Scopus subject areas
Condensed Matter Physics, Materials Chemistry, Inorganic Chemistry, Physical and Theoretical Chemistry
Portal url
https://ucrisportal.univie.ac.at/en/publications/an-investigation-of-polyhedral-deformation-in-two-mixedmetal-diarsenates-srznas2o7-and-bacuas2o7(2f15b50a-e57d-40d7-bbc3-02b49a863250).html