Crystal chemistry of johillerite

Author(s)
Natalya N. Koshlyakova, Natalia V Zubkova, Igor V Pekov, Gerald Giester, Evgeny G. Sidorov
Abstract

Johillerite, an anhydrous arsenate member of the alluaudite group with the idealized crystal chemical formula

A(2)Na

A(1)Cu

MMg

3(TAsO

4)

3, is an abundant mineral in the exhalations of the Arsenatnaya fumarole on the Second scoria cone of the Northern Breakthrough of the Great Tolbachik Fissure Eruption, Kamchatka, Russia. Chemical variations of johillerite from Tolbachik were studied and the crystal structure was solved for three samples that represent different chemical varieties of the mineral. Johillerite forms a continuous solid-solution system with badalovite, Na

2Mg

2Fe

3+(AsO

4)

3, and nickenichite, Na(□,Cu)(□,Ca)(Mg,Fe)

3(AsO

4)

3, and a discontinuous solid solution with bradaczekite, NaCu

4(AsO

4)

3. The major substitution schemes are: (1)

MMg=MCu

2+; (2)

ACu

2++M

2+=ANa

++M

3+; (3)

ANa

++M

2+=

A

0+M

3+; and (4)

ACu

2++2M2+=

A

0+ 2M

3+. The T sites are occupied by As

5+ with only minor admixtures of other constituents (P, V, S, Si). Structurally studied johillerite crystals (monoclinic, C2/c) have the following crystal chemical formulae: (1)

A(2)′Na

0.75

A(1)′Cu

0.85

A(1)Na

0.13

M(1)(Mg

0.91Fe

0.09)

M(2)(Mg

1.60Fe

0.34Cu

0.06)(AsO

4)

3; (2)

A(2)′Na

0.84

A(1)′Cu

0.68

A(1)Na

0.33

M(1)(Mg

0.68Zn

0.32)

M(2)(Mg

0.90Cu

0.62 Fe

0.16Al

0.08)(AsO

4)

3; (3)

A(2)′Na

0.91

A(1)′Cu

0.98

M(1)(Mg

0.74Cu

0.16Zn

0.10)

M(2)(Mg

1.34Cu

0.52Fe

0.14)(AsO

4)

3. Mg and Zn prefer the M(1)O

6 octahedra rather than the M(2)O

6, whereas Fe

3+ and Al

3+ mainly concentrate at the M(2) site.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
Russian Academy of Sciences, Anuchin Research Institute and Museum of Anthropology
Journal
The Canadian Mineralogist
Volume
56
Pages
189-201
No. of pages
13
ISSN
0008-4476
DOI
https://doi.org/10.3749/canmin.1700075
Publication date
03-2018
Peer reviewed
Yes
Austrian Fields of Science 2012
105116 Mineralogy, 105113 Crystallography
Keywords
ASJC Scopus subject areas
Geochemistry and Petrology
Portal url
https://ucrisportal.univie.ac.at/en/publications/52ea0b0c-44cf-4f59-a89b-bbbda394d77d