Using Silica Coated Nanoscale Zerovalent Particles for the Reduction of Chlorinated Ethylenes

Author(s)
Lenka Honetschlägerová, Petra Janouškovcová, Milica Velimirovic-Fanfani, Martin Kubal, Leen Bastiaens
Abstract

The impact of a silica coating on the degradation potential of nanoscale zerovalent iron (nZVI) particles toward a mixture
of chlorinated ethylenes is presented. The newly employed stabilization method for nZVI, based on silica deposition from
saturated sodium silicate water glass, produces nZVI particles with a similar reactivity as non-stabilized particles. Moreover
the removal rate constant kM of trichloroethylene (0.1740 L g−1 d−1 Fe0) and cis-dichloroethylene (0.1045 L g−1 d−1 Fe0)
was significantly improved (almost by a factor of 2) for stabilized nZVI. X-ray photoelectron spectroscopy (XPS) and
Wavelength Dispersive X-ray Fluorescence (WDXRF) analyzes revealed a high durability of silica coating and the coating
left at least half of nZVI surface silica free for reaction for more than 5 weeks. The silica coating did not affect the
surface composition of silica coated nZVI which was confirmed by the very similar distribution of degradation products
and corrosion products (Fe3O4, FeOOH) as was found for non-coated nanoparticles. An enhanced reactivity supplemented
with a stable corrosion properties indicates that silica coated nZVI has potential as an efficient remediation agent toward
chlorinated ethylenes.

Organisation(s)
External organisation(s)
University of Chemistry and Technology, Prague, Flemish Institute for Technological Research (VITO)
Journal
Silicon
Volume
10
Pages
2593–2601
No. of pages
9
ISSN
1876-990X
DOI
https://doi.org/10.1007/s12633-018-9795-2
Publication date
04-2018
Peer reviewed
Yes
Austrian Fields of Science 2012
210001 Nanoanalytics, 104023 Environmental chemistry, 105906 Environmental geosciences, 210004 Nanomaterials
Keywords
ASJC Scopus subject areas
Electronic, Optical and Magnetic Materials
Portal url
https://ucrisportal.univie.ac.at/en/publications/6fc49540-958c-4de6-9f0e-ed04576c0aa8