Synthesis and crystal structure of Cu(II) and Co(II) complexes with the 1,3-dimethylpyrazole-5-carboxylic acid ligand

Author(s)
Zeljko K. Jacimovic, Milica Kosovic, Sladana B. Novakovic, Gerald Giester, Ana Radovic
Abstract

In the reaction of 1,3-dimethylpyrazole-5-carboxylic acid (HL) with M(OAc)2·4H2O, (M = Cu or Co), two novel complexes were prepared, the square-planar [CuL2(H2O)2] and the octahedral [CoL2(MeOH)4]. The crystal structures were determined by single-crystal X-ray diffraction. In both complexes, the deprotonated acid displays monodentate coordination to the metal ions. According to the results of a CSD survey, this is the first structural report on the metal complexes with an N1-substituted pyrazole-5-carboxylic ligand.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
University of Belgrade, Accreditation Body of Montenegro, University of Montenegro
Journal
Serbian Chemical Society. Journal
Volume
80
Pages
867-875
No. of pages
9
ISSN
0352-5139
DOI
https://doi.org/10.2298/JSC140722009J
Publication date
09-2015
Peer reviewed
Yes
Austrian Fields of Science 2012
104015 Organic chemistry, 104011 Materials chemistry, 105113 Crystallography
Keywords
ASJC Scopus subject areas
Chemistry(all)
Portal url
https://ucrisportal.univie.ac.at/en/publications/synthesis-and-crystal-structure-of-cuii-and-coii-complexes-with-the-13dimethylpyrazole5carboxylic-acid-ligand(9b4f46f4-1802-472e-927e-7d646739d199).html