Crystal structure of hexaglycinium dodecaiodotriplumbate

Author(s)
Gayane S. Tonoyan, Gerald Giester, Vahram V. Ghazaryan, Ruben Yu. Chilingaryan, Arthur A. Margaryan, Artak H. Mkrtchyan, Aram M. Petrosyan
Abstract

The crystal structure of hexaglycinium tetra-µ-iodido-octaiodidotriplumbate,
(C2H6NO2)6[Pb3I12] or (GlyH)6[Pb3I12], is reported. The compound crystallizes
in the triclinic space group P1. The [Pb3I12]6- anion is discrete and located
around a special position: the central Pb ion located on the inversion center is
holodirected, while the other two are hemidirected. The supramolecular nature
is mainly based on C—H···I, N—H···I, O—H···I and N—H···O hydrogen
bonds. Dimeric cations of type (A+···A+) for the amino acid glycine are
observed for the first time.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
National Academy of Sciences of the Republic of Armenia
Journal
Acta Crystallographica. Section E: Crystallographic Communications
Volume
80
Pages
916-920
No. of pages
5
ISSN
2056-9890
DOI
https://doi.org/10.1107/S2056989024007606
Publication date
09-2024
Peer reviewed
Yes
Austrian Fields of Science 2012
105116 Mineralogy, 105113 Crystallography
Keywords
ASJC Scopus subject areas
Condensed Matter Physics, General Chemistry, General Materials Science
Portal url
https://ucrisportal.univie.ac.at/en/publications/a616ce6c-c686-4d33-bd6b-51e710fc9c7b