Crystal structures and vibrational spectra of novel compounds with dimeric glycine glycinium cations

Author(s)
V. V. Ghazaryan, Michel Fleck, A.M. Petrosyan
Abstract

The glycinium compounds glycine glycinium tetrafluoroborate (GlyH_Gly_BF4) (I), glycine glycinium perchlorate(GlyH_Gly_ClO4) (II), glycinium tetrafluoroborate (GlyH_BF4) (III), glycinium perchlorate (GlyH_-ClO4) (IV), and glycine glycinium iodide (GlyH_Gly_I) (V) have been synthesized, (I-IV) for the firsttime. The crystal structures could be determined for (I), (II), and (V), the first two represent novel speciesand have therefore been characterized by vibrational spectroscopy as well. Compounds (III) and (IV)proved unstable and are characterized by vibrational spectroscopy only. The results of the redeterminationof (V) are compared with previously reported data. The crystal structures comprise dimeric cations ofthe type (GlyH...Gly) connected to monovalent anions via hydrogen bonds.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
National Academy of Sciences of the Republic of Armenia
Journal
Journal of Molecular Structure
Volume
977
Pages
117-129
No. of pages
13
ISSN
0022-2860
Publication date
2010
Peer reviewed
Yes
Austrian Fields of Science 2012
105113 Crystallography
Portal url
https://ucrisportal.univie.ac.at/en/publications/beed3b9c-739d-4db5-a8fe-2d3bd7e6a2a7