A Pathway for the Growth of Core−Shell Pt−Pd Nanoparticles

Author(s)
Chaitanya K. Narula, Xiofan Yang, Chen Li, Andrew R. Lupini, Stephen J. Pennycook
Abstract

The aging of both Pt−Pd nanoparticles and core−shell Pt−Pd nanoparticles has been reported to result in alloying of Pt with Pd. In comparison to monometallic Pt catalysts, the growth of Pd−Pt bimetallics is slower; however, the mechanism of growth of particles and the mechanism by which Pd improves the hydrothermal durability of bimetallic Pd−Pt particles remains uncertain. In our work on hydrothermal aging of core−shell Pt−Pd nanoparticles, synthesized by solution methods, with varying Pd:Pt ratio of 1:4, 1:1, and 4:1, we compare the growth of core−shell Pt−Pd nanoparticles and find that particles grow by migrating and joining together. The unique feature of the observed growth is that Pd shells from both particles open up and join, thereby allowing the cores to merge. At high temperatures, alloying occurs in good agreement with reports by other workers.

Organisation(s)
Department of Lithospheric Research
External organisation(s)
Oak Ridge National Laboratory , BASF Corporation, National University of Singapore (NUS)
Journal
The Journal of Physical Chemistry Part C (Nanomaterials and Interfaces)
Volume
119
Pages
25114-25121
No. of pages
8
ISSN
1932-7447
DOI
https://doi.org/10.1021/acs.jpcc.5b08119
Publication date
10-2015
Peer reviewed
Yes
Austrian Fields of Science 2012
103042 Electron microscopy
Keywords
ASJC Scopus subject areas
Electronic, Optical and Magnetic Materials, Energy(all), Surfaces, Coatings and Films, Physical and Theoretical Chemistry
Portal url
https://ucrisportal.univie.ac.at/en/publications/a-pathway-for-the-growth-of-coreshell-ptpd-nanoparticles(c1cc71df-e26f-4fa8-852e-d7cd80de5f60).html