Two three-dimensional coordination polymers of lead(II) with iminodiacetate and naphthalene-dicarboxylate anions: Synthesis, characterization and luminescence behavior

Author(s)
Debdoot Hazari, Swapan Kumar Jana, Michel Fleck, Ennio Zangrando, Sudipta Dalai
Abstract

Two lead(II) compounds [Pb3(idiac)3(phen)2(H2O)]·2(H2O) (1) and [Pb(ndc)]n (2), where H2idiac=iminodiacetic acid, phen=1,10-phenanthroline and H2ndc=naphthalene-2,6-dicarboxylic acid, have been synthesized and structurally characterized. Single crystal X-ray diffraction analysis showed that compound 1 is a discrete trinuclear complex (of two-fold symmetry) which evolves to a supramolecular 3D network via π–π interactions, while in compound 2 the naphthalene dicarboxylate anion act as a linker to form a three dimensional architecture, where the anion adopts a bis-(bidentate bridging) coordination mode connecting four Pb(II) centers. The photoluminescence property of the two complexes has been studied.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
Vidyasagar University, Università degli Studi di Trieste
Journal
Journal of Solid State Chemistry
Volume
219
Pages
43-48
No. of pages
6
ISSN
0022-4596
DOI
https://doi.org/10.1016/j.jssc.2014.07.004
Publication date
07-2014
Peer reviewed
Yes
Austrian Fields of Science 2012
104015 Organic chemistry, 104021 Structural chemistry, 105113 Crystallography
Keywords
ASJC Scopus subject areas
Electronic, Optical and Magnetic Materials, Condensed Matter Physics, Ceramics and Composites, Materials Chemistry, Inorganic Chemistry, Physical and Theoretical Chemistry
Portal url
https://ucrisportal.univie.ac.at/en/publications/dcbd0f6f-4521-44e4-a46c-3926963a0703