Mixed salts of amino acids with different anions

Author(s)
V. V. Ghazaryan, Michel Fleck, A.M. Petrosyan
Abstract

Mixed salts of amino acids with different anions are of considerable interest from chemical and structural points of view and also as a source of new materials the properties of which can be controlled by appropriate choice of anions. Four such crystals, L-His2+·Cl-·HSO4- (P212121, Z=4), L-Arg2+·NO3-·ClO4- (d-form, P21, Z=4), L-Arg2+·F-·NO3- (P1, Z=2), 2L-Arg2+·(F-?HF)·3NO3- (P212121, Z=4), have been characterized structurally and by IR and Raman spectra. The hydrogen bond between the carboxyl group and the fluoride ion (2.371(3) Å) in the structure of L-Arg2+·F-·NO3- is among the shortest known O-H?F type hydrogen bonds. The O-H?F hydrogen bond in the structure of 2L-Arg2+·(F-?HF)·3NO3- is even shorter (2.341(2) Å) and thus belongs to the shortest contacts among both ?–??F and F–-?O types hydrogen bonds.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
National Academy of Sciences of the Republic of Armenia
Journal
Journal of Crystal Growth
Volume
362
Pages
182-188
No. of pages
5
ISSN
0022-0248
DOI
https://doi.org/10.1016/j.jcrysgro.2011.09.059
Publication date
2013
Peer reviewed
Yes
Austrian Fields of Science 2012
105116 Mineralogy
Keywords
Portal url
https://ucrisportal.univie.ac.at/en/publications/e33f9700-428a-415f-abac-6f71127f9afe