A rapid method for low-temperature synthesis of the Na analogue of the microporous titanosilicate GTS-1

Author(s)
Stanislav Ferdov, Christian Lengauer, Ognyan Petrov, Vladislav Kostov-Kytin
Abstract

The hydrothermalsynthesis of Grace titanium silicate-1 from a sodium gel at 90°C, without using any organic reactants, was analyzed. In the synthesis process, 3.0 g SiO2 of 12œm particle size was added to a heated solution of 7.1 g NaOH in 40 ml distilled water. The powder x-ray diffraction (XRD) pattern of the synthesized material was collected in a step-scan regime on a PW3710 diffractometer. The primary powder XRD data standardization, interpretation, and standardization of GTS-1 were performed with the PDI package, which provides indexation for the known unit cell parameters and refinements.

Organisation(s)
Department of Mineralogy and Crystallography
External organisation(s)
Bulgarian Academy of Sciences (BAS)
Journal
Journal of Materials Science
Volume
39
Pages
4343-4344
No. of pages
2
ISSN
0022-2461
DOI
https://doi.org/10.1023/B:JMSC.0000033422.72782.99
Publication date
2004
Peer reviewed
Yes
Austrian Fields of Science 2012
1051 Geology, Mineralogy
Portal url
https://ucrisportal.univie.ac.at/en/publications/ecc20590-2d2b-4ee4-b892-a9e89b94b973